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RAS Chemistry & Material ScienceКоординационная химия Russian Journal of Coordination Chemistry

  • ISSN (Print) 0132-344X
  • ISSN (Online) 3034-5499

Synthesis and X-ray Structures of Polymeric Calcium Carboxylates

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PII
10.31857/S0132344X24090084-1
DOI
10.31857/S0132344X24090084
Publication type
Article
Status
Published
Authors
S. N. Melnikov
  • Affiliation: Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences
Volume/ Edition
Volume 50 / Issue number 9
Pages
613-626
Abstract
The reactions of calcium hydroxide with pivalic, 1-naphthoic, and 2-furancarboxylic acids afford the corresponding polymeric calcium carboxylates. Depending on the crystallization conditions, calcium pivalate is isolated as two different coordination polymers: [Ca3(Piv)6(DMF)2]n · 0.635nC6H6 · 0.365nDMF (I) and [Ca(Рiv)(H2O)2.333(DMF)0.666]n · nРiv·0.333H2O (II). The synthesized calcium 1-naphthoate contains coordinated water molecules [Сa(Naph)2(H2O)2]n (III), and calcium furoate [Ca(Fur)2]n (IV) contains no ancillary ligands. The structures of compounds I–IV are determined by X-ray diffraction (XRD) (CIF files CCDC nos. 2342790–2342793, respectively). The structures of compounds I–III are characterized by the 1D polymeric structure, and compound IV is the 3D polymer.
Keywords
кальций карбоксилаты координационные полимеры рентгеноструктурный анализ кристаллическая структура
Date of publication
08.09.2024
Year of publication
2024
Number of purchasers
0
Views
8

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