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RAS Chemistry & Material ScienceКоординационная химия Russian Journal of Coordination Chemistry

  • ISSN (Print) 0132-344X
  • ISSN (Online) 3034-5499

Optimization of the synthesis of salts [V10O28]6– for the preparation of [VO2(DMSO)4](CF3SO3) and its immobilization on polyethylene terephthalate for catalytic applications

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PII
10.31857/S0132344X24120017-1
DOI
10.31857/S0132344X24120017
Publication type
Article
Status
Published
Authors
P. A. Abramov
  • Affiliation: Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences
Volume/ Edition
Volume 50 / Issue number 12
Pages
809-817
Abstract
Aspects of the synthesis and isolation of (Bu4N)3[H3V10O28] (I) and Na6[V10O28] · 18H2O (II) from one reaction mixture are considered. The procedure for the synthesis of compound I is optimized. The reaction of compound I and HSO3CF3 in dimethyl sulfoxide (DMSO) affords complex [VO2(DMSO)4](CF3SO3) (III). A possibility of using complex III for the preparation of catalytically active materials based on polyethylene terephthalate (PET) is shown.
Keywords
декаванадат кристаллическая структура спектры ЯМР 51V
Date of publication
24.12.2024
Year of publication
2024
Number of purchasers
0
Views
12

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