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RAS Chemistry & Material ScienceКоординационная химия Russian Journal of Coordination Chemistry

  • ISSN (Print) 0132-344X
  • ISSN (Online) 3034-5499

Influence of the Aromatic Ligand Nature and Synthesis Conditions on the Structures of the Copper Pentafluorobenzoate Complexes

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PII
10.31857/S0132344X22600503-1
DOI
10.31857/S0132344X22600503
Publication type
Status
Published
Authors
A. S. Chistyakov
  • Affiliation: Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, Moscow, Russia
Volume/ Edition
Volume 49 / Issue number 4
Pages
229-245
Abstract
New pentafluorobenzoate (Рfb) copper complexes with 2,3- and 3,5-lutidine (2,3- and 3,5-Lut, respectively), quinoline (Quin), and 1,10-phenanthroline (Рhen) ([Cu2(MeCN)2(Рfb)4] (I), [Cu(2,3-Lut)2(Pfb)2] (II), [Cu(3,5-Lut)4(Pfb)2] (III), [Cu(Quin)2(Pfb)2] (IV), and [Cu2(Phen)2(Pfb)4] (V)) are synthesized by the newly developed methods and characterized. The unusual heteroanionic pentafluorobenzoate benzoate (Вnz) ionic compound [Cu2(Рhen)2(Рfb)3]+(Рnz)– (VI) is synthesized. It is shown that the four-bridge binuclear metal cage of complex I is not retained in the reactions with various pyridine derivatives. In the case of such α-substituted pyridines as 2,3-lutidine and quinoline, the compositions and structures of the final products of the reactions with copper pentafluorobenzoate are independent of the initial ratio of the reagents and crystallization conditions. It is revealed by the Hirshfeld surface analysis that π···π, C–F···π, C–H···F, and F···F interactions make the major contribution to the stabilization of crystal packings of the synthesized complexes.
Keywords
пентафторбензоаты меди гетероанионные комплексы нековалентные взаимодействия поверхность Хиршфельда
Date of publication
01.04.2023
Year of publication
2023
Number of purchasers
0
Views
10

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