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RAS Chemistry & Material ScienceКоординационная химия Russian Journal of Coordination Chemistry

  • ISSN (Print) 0132-344X
  • ISSN (Online) 3034-5499

Palladium Complexes of Pyrimidine-2-thiones: Synthesis, Structures, and Properties

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PII
10.31857/S0132344X24010063-1
DOI
10.31857/S0132344X24010063
Publication type
Article
Status
Published
Authors
A. S. Kuzovlev
  • Affiliation: Russian Technological University (MIREA)
Volume/ Edition
Volume 50 / Issue number 1
Pages
53-61
Abstract
Complexes [PdL2Cl2] (I) and [PdL2Вr2] (II) (L is 5-acetyl-6-methyl-4-(3-nitrophenyl)-1,2,3,4-tetrahydropyrimidine-2-thione) are synthesized and characterized by spectral methods (1Н, 13С NMR and IR spectroscopy). The crystal structure of complex I is determined (CIF file ССDС no. 2233053) in which the palladium atom is coordinated by two halide ions and two sulfur atoms of two ligands L in a distorted square planar geometry. The catalytic activity of the synthesized palladium(II) complexes in the model epoxidation of allyl alcohol is estimated in comparison with the catalytic activity of the corresponding palladium halides and titanium-containing zeolite TS-1.
Keywords
соединения Биджинелли пиримидин-2-тион палладий катализ эпоксидирование
Date of publication
15.01.2024
Year of publication
2024
Number of purchasers
0
Views
31

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