- PII
- 10.31857/S0132344X24050012-1
- DOI
- 10.31857/S0132344X24050012
- Publication type
- Article
- Status
- Published
- Authors
- Volume/ Edition
- Volume 50 / Issue number 5
- Pages
- 287-295
- Abstract
- Three mono(arylhydrazino)acenaphthenones, that is, mono(2-pyridylhydrazino)acenaphthenone (Py-mhan, L1), mono(4-cyanophenylhydrazino)acenaphthenone (4-CN-Ph-mhan, L2), and mono(3,4,6-trifluoro-2-pyridylhydrazino)acenaphthenone (FPy-mhan, L3), were synthesized by the reaction of acenaphthene quinone with the appropriate arylhydrazine salt; compounds L2 and L3 were obtained for the first time. The subsequent reaction of L1 with nickel chloride in 2 : 1 ratio led to the octahedral complex [Ni(Py-mhan)2] (I), in which Py-mhan acts as a tridentate ligand. All of the prepared compounds were characterized by elemental analysis, IR and 1H NMR spectroscopy, and cyclic voltammetry; the crystal structures of L3 and I were determined by X-ray diffraction.
- Keywords
- аценафтенгидразоны лиганды рентгеноструктурный анализ комплексы синтез никель циклическая вольтамперометрия
- Date of publication
- 15.05.2024
- Year of publication
- 2024
- Number of purchasers
- 0
- Views
- 29
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