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RAS Chemistry & Material ScienceКоординационная химия Russian Journal of Coordination Chemistry

  • ISSN (Print) 0132-344X
  • ISSN (Online) 3034-5499

Synthesis and structures of mixed-ligand lead(II) complexes with decahydro-closo-decaborate anion and azheterocyclic ligands

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PII
10.31857/S0132344X24120052-1
DOI
10.31857/S0132344X24120052
Publication type
Article
Status
Published
Authors
T. М. Garaev
  • Affiliation: Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences
Volume/ Edition
Volume 50 / Issue number 12
Pages
853-859
Abstract
Lead(II) complexation reactions were studied in the presence of salts of the closo-decaborate anion [B10H10]2– and azaheterocyclic ligands 2,2΄-bipyridyl (bipy) or 1,10-phenanthroline (phen) in water and organic solvents (acetonitrile, DMF). Binuclear complex Pb(bipy)2[B10H10] and polymer complex [Pb(phen)[B10H10]] were isolated. The effect of solvents and reagent ratios on the composition and structures of the final complexes was studied. The complex compounds were identified by elemental analysis, IR spectroscopy, and X-ray powder diffraction. The structure of complex [Pb(bipy)2[B10H10]]2 ⋅ 2CH3CN (CCDC no. 2325841) was determined by single-crystal X-ray diffraction.
Keywords
кластерные анионы бора мягкие кислоты комплексообразование рентгеноструктурный анализ
Date of publication
24.12.2024
Year of publication
2024
Number of purchasers
0
Views
7

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