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RAS Chemistry & Material ScienceКоординационная химия Russian Journal of Coordination Chemistry

  • ISSN (Print) 0132-344X
  • ISSN (Online) 3034-5499

Mixed-carboxylate cadmium–europium compounds with monocarboxylic acid anions

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PII
10.31857/S0132344X24120032-1
DOI
10.31857/S0132344X24120032
Publication type
Article
Status
Published
Authors
A. S. Chistyakov
  • Affiliation: Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences
Volume/ Edition
Volume 50 / Issue number 12
Pages
833-843
Abstract
A series of mixed-carboxylate EuCd compounds with 1,10-phenanthroline (phen) and anions of benzoic H(Bz), pentabenzoic H(Pfb), 3,5-dinitrobenzoic H(3,5-Nbz), and 3,5-di-tert-butylbenzoic H(Dtbbz) acids is synthesized: [Eu2Cd2(Phen)2(Рfb)5,4(Bz)4,6].2MeCN (I), [Eu2(H2O)2Cd2(Phen)2(3,5-Nbz)4,1(Bz)5,9] (II) and [EuCd2(EtOH)4(Dtbbz)6(Pfb)] (III). The variation of combinations of aromatic anions makes it possible to reveal the influence of diverse factors on the compositions and structures of new compounds. In the case of benzoate‒pentafluorobenzoate compound I and 3,5-dinitrobenzoate‒benzoate compound II, the aromatic substituents of the anions have nonintegral populations and occupy close positions in the structure of the complex. The combination of the more bulky 3,5-di-tert-butylbenzoate and pentafluorobenzoate anions in compound III results in the formation of a compound with integral populations of the positions of the anions. The synthesized compounds are characterized by XRD, IR spectroscopy, and C, H, N elemental analysis.
Keywords
cмешаннокарбоксилатные комплексы кадмий европий рентгеноструктурный анализ нековалентные взаимодействия
Date of publication
24.12.2024
Year of publication
2024
Number of purchasers
0
Views
10

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